#41: Now Strikes... the Sub-Human; The living Diamond!
Issue 41 of The X-Men (1963) · Feb 1, 1968
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Description
The X-Men fight against the Grotesk, the last survivor of a race (the Sub-Humans) that once had lived in the interior of Earth.
2nd story: Jack O'Diamonds wants Scott Summers to help him with his evil plan and to fight against Professor Xavier. Jack O'Diamonds successfully turns himself into a Living Diamond.